Title: Filtration
1Filtration
By 3A Julia Chan (1) Vivian Chan (4)
Vivian Chan (2) Melody Chan (5)
Haily Chan (3)
2Filtration
In chemistry, filtration is the process of using
a filter to mechanically separate a mixture, to
remove microorganisms from liquid.
- There are many different methods of filtration,
but all aim to attain the separation of two or
more substances. - This is achieved by some form
of interaction between the substance or objects
to be removed and the filter. - The substance
that is to pass through the filter must be a
fluid, i.e. a liquid or gas. The simplest method
of filtration is to pass a solution of a solid
and fluid through a porous interface so that the
solid is trapped, while the fluid passes through.
This principle relies upon the size difference
between the particles making up the fluid, and
the particles making up the solid.
3Gravity Filtration
The filtration we do in the laboratory is called
gravity filtration. - It relies simply on
gravity to effect the filtration. - It is most
useful when removing reasonably large solid
particles from a solution. - The impurity can
be a drying agent or an undesired side product or
leftover reactant
4Folding filter paper
Fold the round piece of filter paper in half
Folded it again and crease to produce a quarter
circle
Make a crease so it becomes a half circle
Place the conical shaped piece of filter paper
into a glass or plastic funnel
Make one outer layer of the paper be separated
from the other three
Make the opening wider by squeezing slightly
together at the creases
5Procedure for the gravity filtration
- 1) Support the filter funnel by a clamp.
- this helps to avoid having the apparatus tip
over - 2) Select the suitable size of filter paper. Fold
it and put it in the funnel. - 3) Carefully pour the solution into the funnel
- (be careful not to overfill the funnel, but you
can keep topping up the funnel) - 4) Prepare a beaker or container to collect the
filtrate
6- We can see the result of the filtration
- a clear, colourless solution is collected in the
beaker - the black residue (charcoal) is trapped on the
fluted filter paper in the funnel. - Note
- Folding the filter paper this way can provide
more surface area for the solution to be
filtered.
filter paper
residue
filtrate
7Vacuum filtration
- It is used to collect a desired solid
- It is faster than gravity filtration,
- the solution and air is forced through the filter
paper by the application of reduced pressure
8- Procedure for vacuum filtration
- Set up an apparatus with a side arm flask, a
filter paper, an adaptor, a Buchner funnel - Connect the side arm flask to a vacuum source
with a thick-walled tubing
Buchner funnel
tubing
9- 3) Wet the paper with a small amount of the
solvent to be used in the filtration. - ?this keeps the paper to stick to the plate
- Turn on the water aspirator.
- 4) Filter the solution Pour the mixture to be
filtered onto the filter paper. The vacuum pull
the liquid rapidly through the filter into flask.
mixture
10- 5) Rinse the cake with a small amount of fresh,
cold solvent - To help remove impurities that were dissolved in
the filtrate - 6) Carefully remove the filter paper and solid
from the funnel. Set the filter cake onto a watch
glass to air dry.
filter cake
solvent
11References
http//en.wikipedia.org/wiki/Filtration http//or
gchem.colorado.edu/hndbksupport/filt/filtration.ht
ml http//www.chem.ucalgary.ca/courses/350/labora
tory/expt03gf.html http//www.chemistry.sjsu.edu/
straus/FILTRATION20htms/GravFilt.htm http//www.
ipfw.edu/chem/266/266Spring04/266n0407.htm