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Lab%20Notebook%20Format%20and%20Rules

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Title: Lab%20Notebook%20Format%20and%20Rules


1
Lab Notebook Format and Rules
2
Introduction
  • The lab notebook is perhaps the single most
    important piece of laboratory equipment.
  • May be entered as evidence in court
  • Poor record keeping results in wasted time
  • Industrial lab records that are inadequate cost
    the company money

3
Notebook Format and Rules
  • Laboratory records are to be kept in a bound
    notebook ( i.e., secured with glue), not a spiral
    notebook or a loose-leaf binder.
  • Pages are consecutively numbered
  • No pages are ever to be removed

4
Notebook Format and Rules
  • All entries are to be made in blue or black ink
  • Everything must be recorded in a neat and tidy
    manner
  • Work must be traceable, intelligible and
    understandable to the notebook author and any
    other persons attempting to duplicate recorded
    information.

5
Notebook Format and Rules
  • It is unacceptable under all circumstances to
    rewrite (or copy over) an experiment in the
    notebook outside of the lab.
  • It is unacceptable to type up portions of the
    notebook and affix them to the notebook.
  • Plan your activities so that you complete all
    information in the laboratory.

6
Notebook Format and Rules
  • Include in your notebook a complete description
    of
  • All work performed
  • All reference material consulted
  • Ideas that you have related to your work.

7
Notebook Format and Rules
  • Graphs, charts, spectra, or spreadsheet analyses
    should be affixed to the pages of the notebook
    with tape or glue.
  • Label the space where the material is to be
    placed with a description or the item and the
    results it contained.
  • Make no notes directly on the inserted material.

8
Notebook Format and Rules
  • On the first page of your notebook are written
    the name of the class, the section, and your
    name.
  • It is also a good idea to put your contact
    information (e.g., your phone number or email
    address) in case your notebook is lost.

9
Notebook Format and Rules
  • Pages 2 and 3 are reserved for a table of
    contents.
  • Write the words Table of Contents at the top of
    these pages.
  • The first entry is to be the table of contents
    itself.
  • An entry is made in the table of contents for
    every experiment when it is begun. The entry
    includes the title of the experiment and the page
    number on which the experiment began.

10
Notebook Format and Rules
  • Immediately following table of contents is a page
    labeled Abbreviations and Other Useful
    Information. These items must be completed
    before the first laboratory session.
  • Only write on the right side pages. The left
    pages are reserved for minor calculations, notes
    of no consequence to the experiment, and notes
    that refer to material found elsewhere in the
    notebook.

11
Notebook Format and Rules
  • If a page is skipped, a large X must be drawn
    across it. The page is then initialed and dated.
  • While frowned upon, you may skip a line as needed
    to separate sections. There should be no unused,
    empty space on a page, except for the printed
    margins.

12
Notebook Format and Rules
  • At the top of each page write the title of the
    experiment that matches in the table of contents.
  • At the bottom of the page place the date that the
    last entry was made on that page, your printed
    name and signature.

13
Notebook Format and Rules
  • If an error is made, draw a single bold
    horizontal line through the error so that it can
    still be read.
  • Write the correct information to the right of the
    incorrect entry and have a short accompanying
    explanation of the reason for exclusion. Never
    use whiteout or completely obliterate the
    incorrect entry.

14
Notebook Format and Rules
  • Do not copy any information from the notebooks of
    former or current students. The only exception is
    when working in a group, and only one member of
    the group recorded the data during the
    experiment. In this case, you must indicate in
    your notebook that the results were copied from
    the other persons notebook. Write the recorders
    name and the page number from which the data were
    copied next to the copied data.

15
Arrangement of Experiments
  • Title This includes the experiments title, your
    name, the name (s) of your lab partner (s), and
    the date the experiment began.

16
Arrangement of Experiments
  • Statement of Purpose Clearly and concisely (two
    or three complete sentences) describe the purpose
    of the experiment, including the general method
    that will be used and anticipated results.

17
Arrangement of Experiments
  • Background Includes more information on the
    goals of the experiment, the methods used and the
    procedure followed.
  • Reference (s) to the procedure that you are using
    following the American Chemical Society
    guidelines.
  • Balanced chemical equations for any chemical
    reactions you will be performing.

18
Arrangement of Experiments
  • A table of the physical properties of all the
    materials (starting materials, solvents, and
    products) with which you will be working.
  • Record any hazardous properties (flammability,
    toxicity, etc.) of the substances that you will
    encounter in the exercise.

19
Arrangement of Experiments
  • Procedural Outline This section is a brief (this
    section should not be more than one or two pages
    long, at most), but complete, description of the
    steps taken to carry out the experiment.
  • Not a rewrite of directions
  • May use a bulleted list

20
Arrangement of Experiments
  • Before beginning the procedural outline, divide
    the pages that will contain the procedure into
    two parts by drawing a vertical line on the page,
    approximately 3/5 of the way across the page from
    the left-hand margin (many notebooks already have
    this line drawn for you). Record the procedure on
    the left-hand side, and any modifications or
    procedural notes on the right-hand side. You do
    not record results on the right-hand side.

21
Arrangement of Experiments
  • Results This section does not need to be
    completed before you come to the lab, but you may
    want to prepare blank tables for recording data.
  • Include
  • Reduced data (e.g., tables), all graphs,
    spreadsheet results, and spectra.
  • Unlike the procedural outline, this and following
    sections may use the right-hand page.

22
Arrangement of Experiments
  • Common Errors
  • Forgetting to leave space for graphs ( a
    hand-drawn graph should take up most, if not all,
    of the page so as to maximize the results
    precision) and other items (e.g., spreadsheet
    output) that will be prepared as part of the
    exercise.

23
Arrangement of Experiments
  • All data should be recorded in this section in
    chronological order.
  • Include
  • All measurements made
  • Important observations
  • All observations are written in passive past
    tense. So instead of I saw the solution turn
    green, one writes, The solution turned green.
  • Personal pronouns (e.g., I, We) are not used
    in scientific writing.

24
Arrangement of Experiments
  • The overuse of personal pronouns is taken as a
    sign of arrogance and the passive is thought to
    sound more objective.
  • Observations are always written in complete
    sentences

25
Arrangement of Experiments
  • Calculations An example of each calculation
    performed to reach the final reported answers
    should be shown with the units clearly shown at
    each step.

26
Arrangement of Experiments
  • Discussion of Conclusions and Error Analysis
    Summarize your results paralleling what you set
    forth in the Statement of Purpose, compare them
    to the expected results and try to place them in
    context of the class. This is not a long section
    it may only be two or three pages long in the
    notebook. The key to a good discussion is to
    concisely cover important points.

27
Arrangement of Experiments
  • Do not write things like
  • I liked this lab
  • This lab went well
  • This lab was successfully completed
  • Do not use personal pronouns.
  • Take your time and put some thought into your
    conclusions.
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