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Physical evidence

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A comparison analysis subjects a suspect specimen and a standard/reference ... GRIM 2. Instrument (Glass Refractive Index Measurement) Automated determination of RI ... – PowerPoint PPT presentation

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Title: Physical evidence


1
Physical evidence
2
Types of physical evidence
  • Biological fluids
  • Blood, semen, saliva
  • Documents
  • Drugs
  • Explosives
  • Fibers
  • Fingerprints
  • Firearms and ammunition
  • Glass
  • Hair
  • Impressions
  • Paint
  • Accelerants
  • Man-made polymeric
  • Soil, vegetative matter
  • Tool marks
  • Powder Residues

3
Comparison
  • A comparison analysis subjects a suspect specimen
    and a standard/reference specimen to the same
    tests and examinations for the ultimate purpose
    of determining whether or not they have a common
    origin.
  • Only tells probability of a common source

4
Individual vs. Class characteristics
  • Evidence which is unique and has a high
    probability of coming from the same source as a
    comparison standard has individual
    characteristics. Example DNA, fingerprints
  • Evidence which has some characteristics which
    make it somewhat likely that it came from the
    same source as a comparison sample possess class
    characteristics.
  • Examples paint color, fiber type, hair, blood
    type

5
Product rule
  • Probability of finding a number of different
    pieces of evidence with class characteristics is
    determined by multiplying individual
    probabilities
  • Williams trial
  • Home carpet 1 in 7,792
  • Car carpet 1 in 3,828
  • Odds of finding two fibers at random 1 in 29
    million

6
Individualizing evidence
  • Even evidence which has class characteristics can
    be individualized by additional factors.
  • Piece of tape was torn from roll found in
    suspects vehicle

7
Properties of samples
  • Physical properties
  • Describe a substance without reference to any
    other substance
  • Weight, volume, color, bp, mp
  • Intensive properties dont depend on sample size
    density, bp, mp
  • Chemical properties
  • Describes the behavior of a substance when it
    reacts or combines with another substance
  • In the presence of Heroin, the Marquis reagent
    turns purple

8
Properties used to analyze glass samples
  • Density weight per unit volume
  • Refractive index velocity of light in vacuum/
    velocity of light in medium
  • Edge thickness
  • Lamination, tempering, etc.
  • Chemical composition is not used

9
Determining density of glass sample
  • Archimedess principle
  • An object immersed in a fluid is buoyed up by a
    force equal to the weight of the displaced fluid.
  • Water has a density of 1 g/cm3 or 1 g/mL
  • Therefore a 2.5 g piece of glass with a volume of
    1mL will weigh only 1.5 g in water
  • Density mass of sample/volume of sample

10
Comparing density by flotation column
  • Place some bromoform (CHBr3, d2.89) in a test
    tube. Add glass fragment and bromobenzene
    (C6H5Br, d1.52) until fragment is suspended.
  • Add known glass fragment and observe whether it
    floats, sinks or is suspended with other glass
    fragment.
  • Both fragments suspended would indicated that
    both had same density.

11
Refractive index
  • A measure of the bending of a ray of light as it
    passes from air into a solid or liquid.
  • Tempered glass will change its refractive index
    as it is annealled (slowly heated and cooled)
  • Immersion method
  • Silicone oil with fragment is heated until Becke
    line disappears.

12
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13
GRIM 2
  • Instrument (Glass Refractive Index Measurement)
  • Automated determination of RI
  • Uses immersion method and analyzes video of glass
    fragment as temperature is altered to determine
    when Becke line disappears.
  • Can determine RI to 0.0002

14
Glass fractures
  • Fracture patterns can be used to determine
  • Whether glass was broken from outside or inside
  • Size of object which pierced glass
  • Velocity of object which pierced glass

15
Radial vs. concentric fractures
  • 3R rule
  • Radial cracks form a Right angle on the Reverse
    side of the force.

16
Soil evidence
  • Soil composition differs in different areas and
    also at different depths.
  • Soil samples can contain
  • Minerals
  • organic matter
  • botanical matter
  • Specific seed and spores
  • man-made substances
  • Dust from inside can also be identifiable
  • Kitchen flour, spices
  • Bathroom powder, make-up

17
Soil analysis
  • Soil properties can be changed with amount of
    moisture present so must first be dried
  • Soil color- observed by smear test
  • Soil pH measured
  • Microscopy
  • Determine soil structure and presence of unusual
    material
  • Minerals
  • Particle size distribution
  • Established by passing through series of nesting
    sieves with decreasing nest size

18
Density Gradient Tubes
  • Formed by layering liquids with decreasing
    density
  • Most dense at bottom, least dense at top
  • Produces distribution pattern which can be
    compared to known sample

Courtyard College Gardens Sports Pitch Crime
Scene
19
Soil sedimentation rate
  • Suspend soil sample in water and observe Visible
    light absorbance over time
  • Graph absorbance values
  • Two sample which have same sedimentation rate
    graphs likely came from a common source
  • Soil is nearly impossible to individualize.
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