In DMSOd6 - PowerPoint PPT Presentation

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In DMSOd6

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You should be able to account for all the peaks (big and small) on the spectrum ... 2,6-di-t-butylphenol Phenol and water peaks in different solvents ... – PowerPoint PPT presentation

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Title: In DMSOd6


1
2,6-di-t-butylphenol Integration
  • In DMSO-d6
  • You should be able to account for all the peaks
    (big and small) on the spectrum

2
2,6-di-t-butylphenol Phenol and water peaks in
different solvents
solvent
phenol
water
phenol
water
solvent
  • Red in CDCl3 Blue in DMSO-d6

3
2,6-di-t-butylphenol Multiplet intensity
deviation from Pascal Triangle
  • Red in CDCl3 Blue in DMSO-d6

4
2,6-di-t-butylphenol Spectrum Artifacts
Probably impurity
  • The main peak is t-butyl peak (normalized to 100)
  • How much is 1JCH coupling strength for the methyl
    group?
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